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#255873 - 02/07/12 04:02 PM Cleaning infected bottles :(
Tiddly Beer Offline
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Registered: 01/02/11
Posts: 46
Loc: Bay Area, CA
A few batches ago, after taking a fermenting bucket apart post-bottling to clean it, I saw that the spigot had a small black spot (outside the beer, but inside the spigot). So basically even though my beer was clean it all flowed past some sort of infection going into the bottles...

I hoped for the best and let it carb and condition, and for the most part the batch came out fine. However, a couple of the bottles picked up that infection. The result (other than a flat or gushing brew) is a black speck stuck to the inside of the bottle.

I've tried dishwasher soap, I've shaken and soaked them for 2 days in PBW and hot water, scrubbed intensely with a bottle brush, soaked with Star-San, and repeated all of the above in various orders. Nothing seems to be able to loosen the infection so I am basically going to have to throw out a few of these bottles.

Should I be worried about the whole case? Many of them came out fine; right carbonation, no off-flavors or aromas, no specks. I PBW soak the bottles after pouring and Star-San them before bottling, but I don't want a speck I can't see now to ruin another batch later. Does anyone have advice or experience fixing an infection of this sort?
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#255875 - 02/07/12 04:09 PM Re: Cleaning infected bottles :( [Re: Tiddly Beer]
Jon_TWR Global Moderator Online   happy
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Plastic or glass bottles? If they're plastic, chuck 'em all. Why risk it?

If they're glass, bake them in the oven on 350° for at least an hour--that should kill any remaining nasties you may have missed in your cleaning.
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#255924 - 02/07/12 09:54 PM Re: Cleaning infected bottles :( [Re: Jon_TWR]
vp09 Global Moderator Offline
Ultimate Mr. Beer Fan
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Registered: 06/23/08
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Loc: Whittier, California
Tiddly Beer,

Jon is right on as always.

Don't throw away your glass. No way that infection (microbes) can stick to glass. It is good stuff and impervious to microbes, infections, what-have-you.

Do you know the difference between clean and sanitized? One means the absence of dirt and grease; the other means that you've reduced microbial levels to negligible.

Point being: Even a spot remaining can be sanitized. Your StarSan will do that no problemo. Or the heat. Be careful if you go that route-- let them cool slowly. Might as well place some potatoes in there too.
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93 Irish Stout (5 gallon LHBS extract kit)
92 Dry Stout (de Malto Seca) Brewing Classic Styles p. 165
91 Oatmeal Stout (McQuakers) BCS p. 169
90 Southern English Brown (Big Ben Brown) Brown Ale: CBS p. 159
89 Southern English Brown (Treacle Treat) Brown Ale: CBS p. 160
88 Mild English Brown BCS, p. 145
87 Southern English Brown BCS, p. 148
86 1750s Brown Brown Ale: CBS p. 154
85 Strong Bitter BCS p. 122
84 Pale Porter CBS Porter, p. 104
83 Special Bitter BCS, p. 119
82 Irish Red Northern Brewers kit
81 Irish Red BCS, p. 129
80 Brown Porter BCS, p. 155
79 Standard Bitter BCS, p. 117
78 Brown; 77 Irish Stout; 76 Dry Stout
75 Brown; 74 Basic Stout; 73 Irish Stout; 72 Porter
69 Smoked Amber Ale; 68 Dane's IPA; 67 Dane's Pale Ale
66 Wormwood 5; 63 Heather Mild
62 Red Ale; 61 LB; 60 Oatmeal Stout 2; 59 Oatmeal Stout
57 Wormwood Rauch 2
53 Wormwood Rauch; 52 Wormwood Peat; 51 Heather Rauch
50 Heather Peat; 49 Wormwood Gruit; 48 Dornbusch's Gruitbier
47 St. Johns Wort & Yarrow
46 Five Herb Gruit: Yarrow, Woodruff, Mugwort, Sweet Gale & Labrador Tea
45 Heather & Sweet Gale; 44 Traditional Gruit: Yarrow, Labrador Tea & Sweet Gale
43 Woodruff, Mugwort, & Bog Myrtle
42 Yarrow & St. Johns Wort; 41 Mugwort & Sweet Gale
40 Sweet Gale; 39 Mugwort; 38 Heather Gruit
37 Yarrow & Bog Myrtle

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#255931 - 02/07/12 11:37 PM Re: Cleaning infected bottles :( [Re: vp09]
Tiddly Beer Offline
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Posts: 46
Loc: Bay Area, CA
Hmm, something is for sure sticking to the glass in each of the infected bottles. There is a black dot (in one bottle it's a line about 1/2 inch long). I don't like the thought of that gunk sitting in the next batch of beer, killed by baking or not, so I would like to get it physically out if possible... Scrubbing with a brush didn't do it, even after soaks in all of the above.

I mentioned above I use PBW to clean and Star-San to sanitize, so yep I am aware of the difference. Unfortunately neither seemed to loosen the spots in the infected bottles. I can try to get a picture if it helps.
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#255932 - 02/07/12 11:42 PM Re: Cleaning infected bottles :( [Re: Tiddly Beer]
vp09 Global Moderator Offline
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Give the glass to your recycling gods if you like-- fresh glass should be easy to pick up-- I'm giving 8 cases to a new brewer tomorrow and gave 14 cases to one a couple months ago-- I bet you have recycling in the bay area -- but just saying, spot or no spot, once you sanitize, the spot is sanitized, thus, not an issue.

I have some scum in the bottom of some of my bottles-- a thin coating I can't remove with either of my brushes-- but I know once it sits in Star San for that time, that it is sanitized.

My advice is toss all your glass and replace, otherwise you will fret on this.

Can you remove it mechanically-- used dental picks are good-- anchor one to a needle-nosed pliers and scrape?

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#255933 - 02/07/12 11:52 PM Re: Cleaning infected bottles :( [Re: vp09]
Tiddly Beer Offline
Beer, beer, beer, tiddly beer!
Active Member

Registered: 01/02/11
Posts: 46
Loc: Bay Area, CA
Originally Posted By: vp09
I have some scum in the bottom of some of my bottles-- a thin coating I can't remove with either of my brushes-- but I know once it sits in Star San for that time, that it is sanitized.

My advice is toss all your glass and replace, otherwise you will fret on this.


I appreciate the advice, I think you pretty much nailed it. Sanitized or not I know I will worry if I can see the damn thing.

Maybe I will just keep the bottles in the back of the closet and get over it someday. Or not, no harm in recycling them later vs sooner.
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Next: [ Oktoberfest Ale ]
Ferm: [ MoreBeer Bock ][ Cinco Cervesa ]
Carb/Cond: [ Feb ROTM: Best Bitter ]
Drink: frown
Gone: [ Coriander Hefeweizen ][ Cherry Wheat ][ Irish Red Ale ][ Oatmeal Stout ][ Nut Brown Ale ][ Kyle's Odiferous Holiday Ale ][ Draught Pub Ale ][ Munich Helles I ][ Señor Chang Vienna Lager ][ American Kolsch ][ Clone: Lagunitas IPA ][ Weak Winter Warmer ][ Milk Stout I ] [ Coriander Hefeweizen ] [ American IPA ][ Oktoberfest Ale ][ Honey Blonde ][ Scottish Wee Heavy I ][ ESB II ][ Low Maintenance Blonde ][ ESB I ][ Black Tower Porter, Creamy Brown UME, Golding ][ Englishman's Nut Brown Ale, Mellow Amber UME, Perle ][ Bavarian Hefeweizen (DME, Perle) ][ Irish Red Ale ][ Sticky Wicket Oatmeal Stout, Creamy Brown UME, Saaz ][ Bavarian Hefeweizen (DME, Saaz) ][ West Coast Pale Ale ]

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#255934 - 02/08/12 12:00 AM Re: Cleaning infected bottles :( [Re: Tiddly Beer]
vp09 Global Moderator Offline
Ultimate Mr. Beer Fan
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Registered: 06/23/08
Posts: 3344
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Thanks!

I see Oatmeal Stout on your signature list-- my favorite -- I don't see anything I don't like on your list ... smile
_________________________
93 Irish Stout (5 gallon LHBS extract kit)
92 Dry Stout (de Malto Seca) Brewing Classic Styles p. 165
91 Oatmeal Stout (McQuakers) BCS p. 169
90 Southern English Brown (Big Ben Brown) Brown Ale: CBS p. 159
89 Southern English Brown (Treacle Treat) Brown Ale: CBS p. 160
88 Mild English Brown BCS, p. 145
87 Southern English Brown BCS, p. 148
86 1750s Brown Brown Ale: CBS p. 154
85 Strong Bitter BCS p. 122
84 Pale Porter CBS Porter, p. 104
83 Special Bitter BCS, p. 119
82 Irish Red Northern Brewers kit
81 Irish Red BCS, p. 129
80 Brown Porter BCS, p. 155
79 Standard Bitter BCS, p. 117
78 Brown; 77 Irish Stout; 76 Dry Stout
75 Brown; 74 Basic Stout; 73 Irish Stout; 72 Porter
69 Smoked Amber Ale; 68 Dane's IPA; 67 Dane's Pale Ale
66 Wormwood 5; 63 Heather Mild
62 Red Ale; 61 LB; 60 Oatmeal Stout 2; 59 Oatmeal Stout
57 Wormwood Rauch 2
53 Wormwood Rauch; 52 Wormwood Peat; 51 Heather Rauch
50 Heather Peat; 49 Wormwood Gruit; 48 Dornbusch's Gruitbier
47 St. Johns Wort & Yarrow
46 Five Herb Gruit: Yarrow, Woodruff, Mugwort, Sweet Gale & Labrador Tea
45 Heather & Sweet Gale; 44 Traditional Gruit: Yarrow, Labrador Tea & Sweet Gale
43 Woodruff, Mugwort, & Bog Myrtle
42 Yarrow & St. Johns Wort; 41 Mugwort & Sweet Gale
40 Sweet Gale; 39 Mugwort; 38 Heather Gruit
37 Yarrow & Bog Myrtle

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#255935 - 02/08/12 12:31 AM Re: Cleaning infected bottles :( [Re: vp09]
Tiddly Beer Offline
Beer, beer, beer, tiddly beer!
Active Member

Registered: 01/02/11
Posts: 46
Loc: Bay Area, CA
Originally Posted By: vp09
I don't see anything I don't like on your list ... smile


Thanks =) I added 2 vanilla beans to the oatmeal stout after a week, looking forward to trying it... I've made a couple of stouts before but this is the first oatmeal*. If your signature is any indication of how good the style is, I don't think this will be my last wink

* edit: first all-grain oatmeal stout, I forgot about the Sticky Wicket


Edited by Tiddly Beer (02/09/12 11:53 PM)
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Next: [ Oktoberfest Ale ]
Ferm: [ MoreBeer Bock ][ Cinco Cervesa ]
Carb/Cond: [ Feb ROTM: Best Bitter ]
Drink: frown
Gone: [ Coriander Hefeweizen ][ Cherry Wheat ][ Irish Red Ale ][ Oatmeal Stout ][ Nut Brown Ale ][ Kyle's Odiferous Holiday Ale ][ Draught Pub Ale ][ Munich Helles I ][ Señor Chang Vienna Lager ][ American Kolsch ][ Clone: Lagunitas IPA ][ Weak Winter Warmer ][ Milk Stout I ] [ Coriander Hefeweizen ] [ American IPA ][ Oktoberfest Ale ][ Honey Blonde ][ Scottish Wee Heavy I ][ ESB II ][ Low Maintenance Blonde ][ ESB I ][ Black Tower Porter, Creamy Brown UME, Golding ][ Englishman's Nut Brown Ale, Mellow Amber UME, Perle ][ Bavarian Hefeweizen (DME, Perle) ][ Irish Red Ale ][ Sticky Wicket Oatmeal Stout, Creamy Brown UME, Saaz ][ Bavarian Hefeweizen (DME, Saaz) ][ West Coast Pale Ale ]

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#258042 - 02/22/12 07:51 AM Re: Cleaning infected bottles :( [Re: Tiddly Beer]
Deucebelow Offline
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Registered: 12/26/11
Posts: 116
Loc: Georgia
Could you soak this stuff in bleach out of curiosity? Maybe put a little layer of bleach down at the bottom and let it sit for a while, and then rinse it out real good?
I mean, I know it's not sanitizing, but maybe it would be useful prior to sanitizing so that you could kill off whatever is residing down in the bottom of that bottle.
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#258047 - 02/22/12 08:15 AM Re: Cleaning infected bottles :( [Re: Deucebelow]
Jon_TWR Global Moderator Online   happy
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Bleach will sanitize, but in order to chemically sanitize a surface, that surface first has to be clean.

So no matter if you're using bleach or starsan, or anything other than heat (either moist or dry for the appropriate time at the appropriate temperatures), it won't be sanitized until you either get that spot off, or heat sanitize it.

To be fair, after all of the soaks you've probably done, it's HIGHLY unlikely that it'll give you any troubles, but there's still a chance.

If you can't get that last bit off, either bake the bottles and forget about it, or just get rid of the questionable bottles and get some new ones.

Good luck either way!
_________________________
CCBBA Yeast Trials

Favorite recipes:
Drunken Druid (Mr. Beer),JPA (All Grain)...there are more that go here, I will add them later.

Wines and Ciders:
House Red
Apfelwein

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#258079 - 02/22/12 09:54 AM Re: Cleaning infected bottles :( [Re: Jon_TWR]
Pudge Global Moderator Offline
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Registered: 01/19/08
Posts: 6438
Loc: West Virginia
Originally Posted By: Jon_TWR
...or just get rid of the questionable bottles and get some new ones...


Yeah, probably the easiest part of your brewing equipment to replace.
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